Applied NMR group

Nuclear Hyperpolarization of Molecular Systems and Nanomaterials. Group leader: Dr. Tomasz Ratajczyk

Publications

2024

  1. Mames A., Gorski A., Jankowska J., Ratajczyk T., Pietrzak M. Light-induced selectivity in an exemplary photodimerization reaction of varied azaanthracenes. Physical Chemistry Chemical Physics (2024) doi:10.1039/D4CP03899A.
  2. Mames, A.; Pietrzak, M.; Ratajczyk, T.Hyperpolarization Methods and Their Applications for the Investigation and Discrimination of Enantiomers in NMRBook chapter in New Developments in NMR No. 34, Physical Principles of Chirality in NMR, Edited by Piotr Garbacz, The Royal Society of Chemistry 2024. https://doi.org/10.1039/9781839169588
  3. Mocny P. , Lin T., Parekh R., Zhao Y., Czarnota M.,  Urbańczyk M., Majidi C.,  Matyjaszewski K., “Selective and Controlled Grafting from PVDF-Based Materials by Oxygen-Tolerant Green-Light-Mediated ATRP”, ACS Applied Materials & Interfaces, 2024, https://doi.org/10.1021/acsami.4c03369
  4. Kołodziejczyk, A., Wroblewska, A., Pietrzak, M., Pyrcz, P., Błaziak, K., Szmigielski, R., „Dissociation constants of relevant secondary organic aerosol components in the atmosphere”, Chemosphere, 2024, 141166.

2023

  1. Bernatowicz, P. Ratajczyk, T., Szymański, S., „Non-uniform orientation of H2 molecules in a magnetic field as a critical condition for the appearance of partially negative NMR lines of o-H2 in hyperpolarization experiments using p-H2”, J. Chem. Phys., 2023, 159, 124304.
  2. Czarnota, Marek, Mames, Adam, Pietrzak, Mariusz, Jopa, Sylwia, Theiß, Franziska, Buntkowsky, Gerd, Ratajczyk, Tomasz, Angew. Chem. Int. Ed. 2023, e202309188.
  3. Stasyuk, N.,  Zakalskiy, A., Nogala, W.,  Gawinkowski, S., Ratajczyk, T.,  Bonarowska M.,  Demkiv, O.,  Zakalska, O., and  Gonchar, M., ” A reagentless amperometric biosensor for creatinine assay based on recombinant creatinine deiminase and N-methylhydantoin-sensitive CoCu nanocomposite”, Sensors & Actuators: B. Chemical, 2023, 393, 134276, https://doi.org/10.1016/j.snb.2023.134276
  4. Mailhiot, S., Mankinen, O., Li, J., Kharbanda, Y., Telkki, V.-V., Urbańczyk, M., “CAT on MOUSE: Control and automation of temperature for single-sided NMR instruments such as NMR-MOUSE”, Magn Reson Chem2023, 1. https://doi.org/10.1002/mrc.5376
  5. Shchukina A., Kasprzak P., Urbańczyk M., Kazimierczuk K, 2023. “The Non-uniform Sampling of 2D NMR Data”, Fast 2D Solution-state NMR: Concepts and Applications, Jean-Nicolas Dumez, Patrick Giraudeau (Book Chapter)
  6. Kharbanda, Y., Mailhiot, S., Mankinen, O., Urbańczyk, M., & Telkki, V.-V. Monitoring cheese ripening by single-sided nuclear magnetic resonance. Journal of Dairy Science, 2023 106(3), 1586–1595. https://doi.org/10.3168/jds.2022-22458
  7. Chwojnowska, E., Grzonka, J., Justyniak, I., Ratajczyk, T., & Lewiński, J. A modular design approach to polymer-coated ZnO nanocrystals. ISCIENCE, 2023 26, 105759.

2022

  1. Jopa S., Mames A., Ratajczyk T., NUCLEAR MAGNETIC RESONANCE SIGNAL ENHANCEMENT BY HYPERPOLARIZATION METHODS
    WITH PARTICULAR FOCUS ON PARAHYDROGEN INDUCED POLARIZATION, Wiadomości Chemiczne, 2022, 76, 11-12
  2. Romero J.A., Putko P., Urbańczyk M., Kazimierczuk K., Zawadzka-Kazimierczuk A., Linear discriminant analysis reveals hidden patterns in NMR chemical shifts of intrinsically disordered proteins, PLOS Computational Biology, 2022, 18(10): e1010258
  3. Kristinaityte K., Mames A., Pietrzak M., Westermair F., Silva W., Gschwind R., Ratajczyk T., and Urbańczyk M., Deeper Insight into Photopolymerization: The Synergy of Time-Resolved Nonuniform Sampling and Diffusion NMR, Journal of the American Chemical Society, 2022, 144, 30, 13938-13945, doi: 10.1021/jacs.2c05944
  4. Cytryniak A., Żelechowska-Matysiak K., Nazaruk E., Bilewicz R., Walczak R., Majka E., Mames A., Bruchertseifer F., Morgenstern A., Bilewicz A, Majkowska-Pilip A., Cubosomal Lipid Formulation for Combination Cancer Treatment: Delivery of a Chemotherapeutic Agent and Complexed α-Particle Emitter 213Bi, Molecular Pharmaceutics, 2022, doi: 10.1021/acs.molpharmaceut.2c00182
  5. Mames A., Jopa S., Pietrzak M., Ratajczyk T., Deactivation of catalysts in simultaneous reversible and irreversible parahydrogen NMR signal enhancement, and the role of co-ligands in the stabilization of the reversible method, RSC Adv., 2022,12, 15986-15991
  6. Kharbanda Y., Urbańczyk M., Zhivonitko V. V., Mailhiot S., Kettunen M. I., Telkki V.-V., Sensitive, Efficient and Portable Analysis of Molecular Exchange Processes by Hyperpolarized Ultrafast NMR. Angew. Chem. Int. Ed.2022, e202203957; Angew. Chem.2022, e202203957.
  7. Pietrzak, M.; Buczyńska, J.; Duus, F.; Waluk, J.; Hansen, P. E. Photoinduced and Ground State Conversions in a Cyclic β-Thioxoketone. RSC Adv. 2022, 12 (2), 681–689.
  8. Woźny, M.; Mames, A.; Ratajczyk, T. Triptycene Derivatives: From Their Synthesis to Their Unique Properties. Molecules. 2022.
  9. Dobkowski, J., Kijak, M., Gawinkowski, S., Karpiuk, E., Pietrzak, M., Sazanovich, I. v., & Waluk, J. Solving the Puzzle of Unusual Excited-State Proton Transfer in 2,5-Bis(6-methyl-2-benzoxazolyl)phenol. The Journal of Physical Chemistry A, 2022.

2021

  1. Ratajczyk, T.; Buntkowsky, G.; Gutmann, T.; Fedorczyk, B.; Mames, A.; Pietrzak, M.; Puzio, Z.; Szkudlarek, P. G. Magnetic Resonance Signal Amplification by Reversible Exchange of Selective PyFALGEA Oligopeptide Ligands Towards Epidermal Growth Factor Receptors. ChemBioChem 2021, 22 (5), 855–860.
  2. Pietrzak, M.; Jopa, S.; Mames, A.; Urbańczyk, M.; Woźny, M.; Ratajczyk, T. Recent Progress in Liquid State Electrochemistry Coupled with NMR Spectroscopy. ChemElectroChem 2021, 8 (22), 4181–4198.
  3. Nawrocka, E. K.; Urbańczyk, M.; Koziński, K.; Kazimierczuk, K. Variable-Temperature NMR Spectroscopy for Metabolite Identification in Biological Materials. RSC Adv. 2021, 11 (56), 35321–35325.
  4. Kristinaityte, K.; Urbańczyk, M.; Mames, A.; Pietrzak, M.; Ratajczyk, T. Photoreactivity of an Exemplary Anthracene Mixture Revealed by NMR Studies, Including a Kinetic Approach. Molecules . 2021.
  5. Kasprzak, P.; Urbańczyk, M.; Kazimierczuk, K. Clustered Sparsity and Poisson-Gap Sampling. J. Biomol. NMR 2021, 75 (10), 401–416.
  6. Mames, A.; Pietrzak, M.; Bernatowicz, P.; Kubas, A.; Luboradzki, R.; Ratajczyk, T. NMR Crystallography Enhanced by Quantum Chemical Calculations and Liquid State NMR Spectroscopy for the Investigation of Se-NHC Adducts**. Chem. – A Eur. J. 2021, 27 (66), 16477–16487.

2020

  1. Dolinska, J.; Holdynski, M.; Pieta, P.; Lisowski, W.; Ratajczyk, T.; Palys, B.; Jablonska, A.; Opallo, M. Noble Metal Nanoparticles in Pectin Matrix. Preparation, Film Formation, Property Analysis, and Application in Electrocatalysis. ACS Omega 2020.
  2. Mames, A.; Gołowicz, D.; Pietrzak, M.; Kazimierczuk, K.; Szymański, S.; Ratajczyk, T. Blue-Shift Hydrogen Bonds in Silyltriptycene Derivatives: Antibonding Σ* Orbitals of the Si−C Bond as Effective Acceptors of Electron Density. ChemPhysChem 2020.
  3. Ostapko, J.; Gorski, A.; Buczyńska, J.; Golec, B.; Nawara, K.; Kharchenko, A.; Listkowski, A.; Ceborska, M.; Pietrzak, M.; Waluk, J. Towards More Photostable, Brighter, and Less Phototoxic Chromophores: Synthesis and Properties of Porphyrins Functionalized with Cyclooctatetraene. Chem. – A Eur. J. 2020, 26 (70), 16666–16675.
  4. Olszowska-Łoś, I.; Ratajczyk, T.; Pieta, I. S.; Siejca, A.; Niedziółka-Jönsson, J.; Leśniewski, A. In Situ Interactions of Eu(TTA)3(H2O)2 with Latent Fingermark Components—A Time-Gated Visualization of Latent Fingermarks on Paper. Anal. Chem. 2020, 92 (23), 15671–15678.
  5. Cytryniak, A.; Nazaruk, E.; Bilewicz, R.; Górzyńska, E.; Żelechowska-Matysiak, K.; Walczak, R.; Mames, A.; Bilewicz, A.; Majkowska-Pilip, A. Lipidic Cubic-Phase Nanoparticles (Cubosomes) Loaded with Doxorubicin and Labeled with 177Lu as a Potential Tool for Combined Chemo and Internal Radiotherapy for Cancers. Nanomaterials . 2020.

2019

  1. Mames, A.; Osior, A.; Szkudlarek, P. G.; Pietrzak, M.; Szymański, S.; Ratajczyk, T. Synthesis and Structural Characterization of Exemplary Silyl Triptycenes. New J. Chem. 2019, 43 (20).
  2. Hadjiali, S.; Savka, R.; Plaumann, M.; Bommerich, U.; Bothe, S.; Gutmann, T.; Ratajczyk, T.; Bernarding, J.; Limbach, H.-H.; Plenio, H.; Buntkowsky, G. Substituent Influences on the NMR Signal Amplification of Ir Complexes with Heterocyclic Carbene Ligands. Appl. Magn. Reson. 2019, 50 (7).
  3. Tulewicz, A.; Wolska-Pietkiewicz, M.; Jędrzejewska, M.; Ratajczyk, T.; Justyniak, I.; Lewiński, J. Towards Extended Zinc Ethylsulfinate Networks by Stepwise Insertion of Sulfur Dioxide into Zn−C Bonds. Chem. – A Eur. J. 2019.
  4. Dobkowski, J.; Gorski, A.; Kijak, M.; Pietrzak, M.; Redeckas, K.; Vengris, M. Combined Picosecond Time-Resolved UV–Vis and NMR Techniques Used for Investigation of the Excited State Intramolecular Triplet–Triplet Energy Transfer. J. Phys. Chem. A 2019, 123 (32), 6978–6985.
  5. Gołowicz, D.; Kazimierczuk, K.; Urbańczyk, M.; Ratajczyk, T. Monitoring Hydrogenation Reactions Using Benchtop 2D NMR with Extraordinary Sensitivity and Spectral Resolution. ChemistryOpen 2019, 8 (2).
  6. Asztemborska, M.; Ceborska, M.; Pietrzak, M. Complexation of Tropane Alkaloids by Cyclodextrins. Carbohydr. Polym. 2019, 209, 74–81.

2018

  1. Grala, A.; Wolska-Pietkiewicz, M.; Wróbel, Z.; Ratajczyk, T.; Kuncewicz, J.; Lewiński, J. Remarkable Water-Soluble ZnO Nanocrystals: From “click” Functionalization to a Supramolecular Aggregation Enhanced Emission Phenomenon. Mater. Chem. Front. 2018, 2 (6).

2017

  1. Cieślak, A. M.; Janeček, E.-R.; Sokołowski, K.; Ratajczyk, T.; Leszczyński, M.K.; Scherman, O. A.; Lewiński, J. Photo-Induced Interfacial Electron Transfer of ZnO Nanocrystals to Control Supramolecular Assembly in Water. Nanoscale 2017, 9 (42).
  2. Szupiluk, A.; Bernatowicz, P.; Ratajczyk, T.; Szymanski, S. Frozen Rotation of the Ammonium Group Observed for the First Time in Liquid-Phase NMR Spectra. J. Phys. Chem. A 2017, 121 (2).